Further syntheses is described towards the reduced form of the CH2 phosphonate analogue of DXP, and to a compound related to fosmidomycin. Chapter 3 describes fluorine’s stereoelectronic influence in determining the conformations of fluoromethyl containing organic compounds through n/ conjugation and gauche effects. Solid state evidence for the influence of these effects is presented through the first X ray crystallographic data of fluoromethylaromatics and fiuoroethylamides respectively.
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